M. Yashwanth Kumar,
T. Vijayakumar,
R. Dhanasekaran,
- Research Scholar, Department of Mechanical Engineering, Koneru Lakshmaiah Education Foundation, Green Fields, Vaddeswaram, Guntur, Andhra Pradesh, India
- Associate Professor, Department of Mechanical Engineering, Koneru Lakshmaiah Education Foundation, Green Fields, Vaddeswaram, Guntur, Andhra Pradesh, India
- Professor, Department of Mechanical Engineering, Adhiyamaan College of Engineering, Hosur, Tamil Nadu, India
Abstract
This work investigates the mechanical characteristics of Al2024-Al2O3-Graphite reinforced monolithic and hybrid composites fabricated by the stir casting method. Exploratory work involved the fabrication of monolithic composites with varying Al2O3 contents (5-8 wt%) and hybrid composites with the ratios of Al2O3 (2-6 wt%) and Graphite (1-3 wt%) in matrix Al2024. For improving their dispersion, preheated reinforcement particles were introduced in matrix alloy at controlled stirring rates. A homogeneous particle distribution with a clustering coefficient below 0.15 and an appropriate mean inter-particle spacing of 12.5 ± 2.3 μm was validated by quantitative microstructural analysis using image analysis software. Mechanical tests were done on the produced composites in order to analyse their mechanical and tribological characteristics. The development of graphite tribofilms during sliding wear was validated by post-wear surface characterization using SEM-EDS mapping and Raman spectroscopy. The results demonstrate that hybrid composites have enhanced mechanical and tribological properties relative to both the reference Al2024 alloy and monolithic composites. Surprisingly Hardness of hybrid composites, Sample 3 (Al2024 + 2% Al2O3+ 1% Graphite) and Sample 4 (Al2024 + 6% Al2O3 + 3% Graphite) were highly improved with samples showing 28% and 35% improvements in hardness, respectively, over the reference alloy. Besides, hybrid composite wear resistances were better than those of monolithic composites, which testified to the synergistic reinforcement effect of Al2O3 and Graphite. Comparative study with recent literature demonstrates that the current hybrid composites achieve greater performance compared to Al₂O₃-graphene (48% hardness increase vs. our 35%) and Al₂O₃-B₄C systems reported in high-impact journals. Yet, attempts at incorporating increased reinforcement levels (Al2O3 9% and Graphite 5%) failed because of agglomeration problems. The findings imply that hybrid composites provide an affordable option with improved mechanical properties and more effective alternative to monolithic composites reinforced by Al2O3 alone
Keywords: Al2024, Al2O3, Graphite, Tensile strength, Hardness, Wear rate. SEM.
[This article belongs to Special Issue under section in Journal of Polymer & Composites (jopc)]
M. Yashwanth Kumar, T. Vijayakumar, R. Dhanasekaran. Mechanical & Tribological Characterization of Al2024-Alumina-Graphite Reinforced Monolithic and Hybrid Composites. Journal of Polymer & Composites. 2026; 14(01):823-836.
M. Yashwanth Kumar, T. Vijayakumar, R. Dhanasekaran. Mechanical & Tribological Characterization of Al2024-Alumina-Graphite Reinforced Monolithic and Hybrid Composites. Journal of Polymer & Composites. 2026; 14(01):823-836. Available from: https://journals.stmjournals.com/jopc/article=2026/view=236084
References
- Srikhar K, Omprakash B. Evaluation of mechanical behaviour of aluminium 2024 composites with boron nitride. Mater Today Proc. 2024. doi:10.1016/j.matpr.2024.05.057.
- Vinod Kumar, Reddappa HN, Chandrashekar A, Paruti B. Stir-cast Al2024 based composite reinforced with boron carbide and graphene particles: Mechanical and dry sliding wear characteristics. Eng Rep. 2024;6(10). doi:10.1002/eng2.12850.
- Sahoo B, Paul J, Sharma A. Mechanical and Tribological Behaviour of Surface Graphitised Al-1100 Alloy. 2024;12(4):139. doi:10.3390/lubricants12040139.
- Kambaiah R, Suresh R, Nagaral M, Auradi V, Anjinappa C, Garse K, Wodajo AW. Mechanical‐wear behavior and microstructure analysis of Al2214 alloy with B4C and graphite particles hybrid composites. Eng Rep. 2024;e12876. doi:10.1002/eng2.12876.
- Sameezadeh M, Emamy M, Farhangi H. Effects of particulate reinforcement and heat treatment on the hardness and wear properties of AA 2024-MoSi2 nanocomposites. Mater Des. 2011;32(4):2157-2164. doi:10.1016/j.matdes.2010.11.037.
- Manjunath YJ, Thirthaprasada HP, Chandrashekar A, et al. Tensile and wear properties of repetitive corrugation and straightened Al 2024 alloy: an experimental and RSM approach. Mater Res Express. 2021;8:126512.
- Nagaral M, Deshapande RG, Boppana SB, Dayanand S, Anilkumar MR. Mechanical and Wear characterization of ceramic boron carbide-reinforced Al2024 alloy metal composites. J Bio Tribo Corros.2021;7:19.
- Ashwin A, Hari Lakshman RB, Chand Swaroop CB, Vignesh M, Vaira Vignesh R, Padmanaban R. Predicting the Wear rate of aluminium alloy AA2024-T351 using hybrid linear function and radial basis function. IOP Conf Ser Mater Sci Eng. 2019;561:012046.
- Varol T, Canakci A. Synthesis and characterization of nanocrystalline Al 2024–B4C composite powders by mechanical alloying. Philos Mag Lett. 2013;93(6):339-345.
- Jafari M, Enayati MH, Abbasi MH, Karimzadeh F. Compressive and wear behaviors of bulk nanostructured Al2024 alloy. Mater Des. 2010;31:663–669. doi:10.1016/j.matdes.2009.08.020.
- Jadhav PR, Nagaral M, Rachoti S, Harti JI. Impact of boron carbide and graphite dual particulates addition on wear behavior of A356 alloy metal matrix composites. J Met Mater Miner. 2020;30(4):106-112. doi:10.55713/jmmm.v30i4.642.
- Radhika N, Subramanian R, Venkat Prasat S, Anandavel B. Dry sliding wear behaviour of aluminium/alumina/graphite hybrid metal matrix composites. Ind Lubr Tribol. 2012;64(6):359-366. doi:10.1108/00368791211262499.
- Sahoo B, Kumar R, Joseph J, Sharma A, Paul J. Preparation of aluminium 6063-graphite surface composites by an electrical resistance heat assisted pressing technique. Surf Coat Technol. 2017;309:563-572. doi:10.1016/j.surfcoat.2016.12.011.
- Baradeswaran A, Perumal AE. Wear and mechanical characteristics of Al 7075/graphite composites. Compos Part B Eng. 2014;56:472–476. doi:10.1016/j.compositesb.2013.08.073.
- Kok M. Production and mechanical properties of Al2O3 particle-reinforced 2024 aluminium alloy composites. J Mater Process Technol. 2005;161:381–387.
- Mazahery A, Ostadshabani M. Investigation on mechanical properties of nano-Al2O3-reinforced aluminum matrix composites. J Compos Mater. 2011; 45(24): 2579-2586. doi:10.1177/0021998311401111.
- Suresh S, Shenbaga Vinayaga Moorthi N, Vettivel SC, Selvakumar N, Jinu GR. Effect of graphite addition on mechanical behavior of Al6061-TiB2 hybrid composites using acoustic emission. Mater Sci Eng A. 2014;612:16-27. doi:10.1016/j.msea.2014.06.024.
- Ramesh A, Prakash JN, Shiva Shankare Gowda AS, Appaiah S. Comparison of the mechanical properties of Al6061-albite and Al6061-graphite metal matrix composites. J Miner Mater Charact Eng. 2009;8(2):93-106.
- Somayaji A, Nagaral M, Anjinappa C, et al. Influence of graphite particles on the mechanical and wear behavior of Al6082 alloy composites. ACS Omega. 2023;8(30):26828-26836. doi:10.1021/acsomega.3c01313.
- Lokesh T, Mallik US. Dry sliding wear behavior of Al-Gr-SiC hybrid metal matrix composites by Taguchi techniques. Mater Today Proc. 2017;4:11175-11180.
- Sundriyal P, Lal PL. Enhancement of mechanical properties of graphite particulate aluminium metal matrix composites by magnesium addition. Mater Today Proc. 2017;4:9481-9486. doi:10.1016/j.matpr.2017.06.208.
- Zebarjad SM, Sajjadi SA. Dependency of physical and mechanical properties of mechanical alloyed Al– Al2O3 composite on milling time. Mater Des. 2007;28:2113–2120. doi:10.1016/j.matdes.2006.05.020.
- Rahimian M, Ehsani N, Parvin N, Baharvandi HR. The effect of sintering temperature and the amount of reinforcement on the properties of Al– Al2O3 Mater Des. 2009;30:3333–3337. doi:10.1016/j.matdes.2008.11.027.
- Nagaral M, Auradi V, Ravishankar MK. Mechanical behaviour of aluminium 6061 alloy reinforced with Al2O3 & graphite particulate hybrid metal matrix composites. Int J Res Eng Technol. 2013;1(2):193-198.
- Kikuchi, Melissa & Sucaria, Rogério & Souza, Gismar & Beltrami, Monica. (2017). The influence of specimen surface roughness on tensile testing results. 26678/ABCM.COBEM2017.COB17-1942.
- Mohammed, A., et al. “Tribological Behavior of Aluminum Hybrid Nanocomposites Reinforced with Alumina and Graphene Oxide.” Materials, vol. 15, 2022. doi:10.3390/ma15030865
- Daha, M. A., et al. “Mechanical and Tribological Characterization of a Novel Hybrid Aluminum/ Al2O3/RGO Composite Synthesized Using Powder Metallurgy.” Journal of Materials Engineering and Performance, 2021. doi:10.1007/S11665-021-05547-0
- Shivaprakash, S., et al. “Mechanical characterization of alumina and graphite dual particulates reinforced hybrid aluminum alloy (Al2219) matrix composites.” Research on engineering structures & materials, 2024. doi:10.17515/resm2024.328me0621rs
- Venkatappa, V. C. “Study on Mechanical, Wear and Thermal Properties of Al2O3/Graphite Reinforced AA2024 Aluminum Alloy Based Metal Matrix Composites.” International Journal For Science Technology And Engineering, 2022. doi:10.22214/ijraset.2022.48218
- Prusov, E. S., Shabaldin, I. V., & Deev, V. B. “Quantitative Characterization of the Microstructure of in Situ Aluminum Matrix Composites.” Journal of Physics: Conference Series, 2021. doi:10.1088/1742-6596/2131/4/042040

Journal of Polymer & Composites
| Volume | 14 |
| Special Issue | 01 |
| Received | 07/09/2025 |
| Accepted | 19/09/2025 |
| Published | 17/01/2026 |
| Publication Time | 132 Days |
Login
PlumX Metrics