Dynamic Mechanical Analysis of Carbon Fiber Reinforced Polymer Composites

Year : 2025 | Volume : 13 | Special Issue 05 | Page : 386 393
    By

    G Ashwin Prabhu,

  • Rajesh Sudhakar,

  • R Sathishkumar,

  • G M Lionus Leo,

  • Aarsath Crisple B,

  • Abdul Rahman A H,

  1. Assistant Professor, Department of Mechanical Engineering, St. Joseph’s College of Engineering, Old Mahabalipuram Road, Chennai, Tamil Nadu, India
  2. Professor, Department of Mechanical Engineering, Meenakshi College of Engineering, 12, Vembuli Amman Koil Street, West K. K. Nagar, Chennai, Tamil Nadu, India
  3. Assistant Professor, Department of Artificial intelligence and Data Science, St. Joseph’s College of Engineering, Old Mahabalipuram Road, Chennai, Tamil Nadu, India
  4. Associate Professor, Department of Mechanical Engineering, St. Joseph’s College of Engineering, Old Mahabalipuram Road, Chennai, Tamil Nadu, India
  5. UG Scholar, Department of Mechanical Engineering, St. Joseph’s College of Engineering, Old Mahabalipuram Road, Chennai, Tamil Nadu, India
  6. UG Scholar, Department of Mechanical Engineering, St. Joseph’s College of Engineering, Old Mahabalipuram Road, Chennai, Tamil Nadu, India

Abstract

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This study investigates the thermal decomposition and mechanical properties of Fiber-Reinforced Polymer Composites (FRPCs) using Dynamic Mechanical Analysis (DMA). The research focuses on improving the recycling and recovery process of Carbon Fiber-Reinforced Polymers (CFRPs), addressing environmental concerns regarding their disposal. By analyzing the effects of different heating rates (5°C and 10°C per minute) and atmospheric conditions (nitrogen, oxygen, and a combination of both), the study identifies optimal parameters for maximizing fiber retention while effectively degrading the polymer matrix. The experimental procedure involved heating CFRP samples to 420°C in a nitrogen atmosphere, facilitating the decomposition of phenolic resin while maintaining fiber integrity. The most efficient recovery method was found at 540°C under oxygen, where the epoxy resin degraded completely while preserving the filament structure. The glass transition temperature (Tg), storage modulus (E’), loss modulus (E’’), and damping factor (Tan δ) were examined to assess the thermal and mechanical stability of different CFRP laminates. Among the tested laminates, Laminate 1 (0° stacking sequence) demonstrated superior mechanical performance, exhibiting the highest storage modulus (20,000 MPa), lowest damping factor (0.11), and highest Tg (240°C), making it ideal for high-performance applications such as automotive and aerospace industries. The results confirm that optimized stacking sequences enhance both mechanical strength and thermal stability, ensuring the structural integrity of CFRP composites under varying conditions. The research underscores the importance of thermal optimization in composite recycling, providing a pathway for enhanced reuse and waste management of carbon fiber materials.

Keywords: Dynamic Mechanical Analysis, Carbon Fiber-Reinforced Polymer, Thermal Decomposition, Glass Transition Temperature, Reclaimed Carbon Fibers.

[This article belongs to Special Issue under section in Journal of Polymer and Composites (jopc)]

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How to cite this article:
G Ashwin Prabhu, Rajesh Sudhakar, R Sathishkumar, G M Lionus Leo, Aarsath Crisple B, Abdul Rahman A H. Dynamic Mechanical Analysis of Carbon Fiber Reinforced Polymer Composites. Journal of Polymer and Composites. 2025; 13(05):386-393.
How to cite this URL:
G Ashwin Prabhu, Rajesh Sudhakar, R Sathishkumar, G M Lionus Leo, Aarsath Crisple B, Abdul Rahman A H. Dynamic Mechanical Analysis of Carbon Fiber Reinforced Polymer Composites. Journal of Polymer and Composites. 2025; 13(05):386-393. Available from: https://journals.stmjournals.com/jopc/article=2025/view=0


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References

  1. Menard KP, Menard NR (2015) Dynamic Mechanical Analysis in the Analysis of Polymers and Rubbers. Encyclopedia of Polymer Science and Technology 1–33
  2. Saba N, Jawaid M, Alothman OY, Paridah MT (2016) A review on dynamic mechanical properties of natural fibre reinforced polymer composites. Construction and Building Materials 106:149–159
  3. Jones D (1999) Dynamic mechanical analysis of polymeric systems of pharmaceutical and biomedical significance. International Journal of Pharmaceutics 179:167–178
  4. Rieger J (2001) The glass transition temperature Tg of polymers—Comparison of the values from differential thermal analysis (DTA, DSC) and dynamic mechanical measurements (torsion pendulum). Polymer Testing 20:199–204
  5. Kister G, Dossi E (2015) Cure monitoring of CFRP composites by dynamic mechanical analyser. Polymer Testing 47:71–78
  6. Murugapoopathi, S., Ashwin Prabhu, G., Chandrasekar, G. et al. Fabrication and Characterisation of Saw Dust Polymer Composite. J. Inst. Eng. India Ser. D (2023).
  7. Venkategowda T, Manjunatha LH, Anilkumar PR (2022) Dynamic mechanical behavior of natural fibers reinforced polymer matrix composites – A review. Materials Today: Proceedings 54:395–401
  8. Muna II, Mieloszyk M (2021) Temperature Influence on Additive Manufactured Carbon Fiber Reinforced Polymer Composites. Materials 14:6413
  9. Gu Y, Li M, Wang J, Zhang Z (2010) Characterization of the interphase in carbon fiber/polymer composites using a nanoscale dynamic mechanical imaging technique. Carbon 48:3229–3235
  10. Stark W (2013) Investigation of the curing behaviour of carbon fibre epoxy prepreg by Dynamic Mechanical Analysis DMA. Polymer Testing 32:231–239
  11. Morampudi P, Namala KK, Gajjela YK, Barath M, Prudhvi G (2021) Review on glass fiber reinforced polymer composites. Materials Today: Proceedings 43:314–319
  12. Pramanik A, Basak AK, Dong Y, Sarker PK, Uddin MS, Littlefair G, Dixit AR, Chattopadhyaya S (2017) Joining of carbon fibre reinforced polymer (CFRP) composites and aluminium alloys – A review. Composites Part A: Applied Science and Manufacturing 101:1–29.
  13. Subramanian PM, Balamurugan L, Ashwin Prabhu G. Novel approaches in developing sustainable and cost-effective semi-active suspension systems for smart vehicles—A review. Proceedings of the Institution of Mechanical Engineers, Part E: Journal of Process Mechanical Engineering. 2024;0(0).
  14. Saba N, Jawaid M (2018) A review on thermomechanical properties of polymers and fibers reinforced polymer composites. Journal of Industrial and Engineering Chemistry 67:1–11
  15. Wielage B, Lampke T, Utschick H, Soergel F (2003) Processing of natural-fibre reinforced polymers and the resulting dynamic–mechanical properties. Journal of Materials Processing Technology 139:140–14
  16. Faruk O, Bledzki AK, Fink H-P, Sain M (2013) Progress Report on Natural Fiber Reinforced Composites. Macromol Mater Eng 299:9–26
  17. Selvam, R., Karunamoorthy, L., & Arunkumar, N (2017) Investigation on performance of abrasive water jet in machining hybrid composites. ater. Manuf. Process. 32(6): 700-706
  18. Karaş B, Smith PJ, Fairclough JPA, Mumtaz K (2022) Additive manufacturing of high density carbon fibre reinforced polymer composites. Additive Manufacturing 58:103044.
  19. Prabhu, G. A., Muninathan, K., Kanna, O. L., Monish, G., & Arun, S. R. (2020, September). Static Analysis of Aluminum 6063 Alloy for Steering Knuckle Application in Student Formula Car. In IOP Conference Series: Materials Science and Engineering (Vol. 923, No. 1, p. 012007). IOP Publishing.
  20. Wang K, Young B, Smith ST (2011) Mechanical properties of pultruded carbon fibre-reinforced polymer (CFRP) plates at elevated temperatures. Engineering Structures 33:2154–2161.
  21. Prabhu, G. A., Sathishkumar, N., Pravinkumar, K., Kumar, P. M., Balasubramanian, T., & Sudharsan, P. L. (2021). Heat treatment and analysis of nickel super alloy for gas turbine applications. Materials Today: Proceedings, 39, 1417-1421.
  22. Zhang J, Chevali VS, Wang H, Wang C-H (2020) Current status of carbon fibre and carbon fibre composites recycling. Composites Part B: Engineering 193:108053
  23. Wong KH, Pickering SJ, Rudd CD (2010) Recycled carbon fibre reinforced polymer composite for electromagnetic interference shielding. Composites Part A: Applied Science and Manufacturing 41:693– 702
  24. Prabhu, G.A., Tembhekar, T.D., Gopal, V. et al. Utilizing Machine Learning for Optimizing Composite Materials Derived from Leather Trimming and HDPE Waste. J. Inst. Eng. India Ser. D (2025).
  25. Feih S, Mouritz AP (2012) Tensile properties of carbon fibres and carbon fibre–polymer composites in fire. Composites Part A: Applied Science and Manufacturing 43:765–772
  26. Carolan D, Ivankovic A, Kinloch AJ, Sprenger S, Taylor AC (2016) Toughened carbon fibre-reinforced polymer composites with nanoparticle-modified epoxy matrices. J Mater Sci 52:1767–1788
  27. Stalin, B., Arivukkarasan, S., & Prabhu, G. A. (2015). Microstructure and mechanical properties evaluation of aluminium matrix reinforced with tungsten carbide and silicon carbide. International Journal of Applied Engineering Research, 10(55), 3994-3999.
  28. Choi J-H, Nam Y-W, Jang M-S, Kim C-G (2018) Characteristics of silicon carbide fiber-reinforced composite for microwave absorbing structures. Composite Structures 202:290–295.
  29. Ryu Z, Zheng J, Wang M, Zhang B (2002) Preparation and characterization of silicon carbide fibers from activated carbon fibers. Carbon 40:715–720
  30. Prabhu, G. A., Selvam, R., & Kumar, K. M. (2024). Enhancing the Mechanical Properties of Basalt Fiber and Stainless Steel Wire Mesh Composites Incorporating Fire Retardants Through Response Surface Methodology Optimization. Fibers and Polymers, 25(4), 1443-1455.

Special Issue Subscription Original Research
Volume 13
Special Issue 05
Received 12/02/2025
Accepted 22/03/2025
Published 23/07/2025
Publication Time 161 Days

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