Investigations into the Mechanical and Thermal Properties of Fe3C Compound: A Comprehensive Analysis

[{“box”:0,”content”:”[if 992 equals=”Open Access”]

n

Open Access

n

[/if 992]n

n

Year : April 1, 2024 at 12:55 pm | [if 1553 equals=””] Volume : [else] Volume :[/if 1553] | [if 424 equals=”Regular Issue”]Issue[/if 424][if 424 equals=”Special Issue”]Special Issue[/if 424] [if 424 equals=”Conference”][/if 424] : | Page : –

n

n

n

n

n

n

By

n

    n t

    [foreach 286]n

    n

    Purushotham Endla, Endla AkhilBalaji

  1. [/foreach]

    n

n

n[if 2099 not_equal=”Yes”]n

    [foreach 286] [if 1175 not_equal=””]n t

  1. Associate Professor, Student, Department of Physics, School of Sciences, Computer Science and Engineering, Telangana, Telangana, India, India
  2. n[/if 1175][/foreach]

[/if 2099][if 2099 equals=”Yes”][/if 2099]nn

n

Abstract

nExploration of mechanical properties of Fe3C powder using Williamson-Hall analysis by using Mechanical alloying technique. The primary objective of this study is to investigate the lattice strain (LS) and nanocrystalline size (CS) in an Fe3C produced from powder using the Mechanical Alloying Method (MAM). By the repeated mechanical crushing, the LS created by MAM is expected to decrease while the CS is anticipated to reduce the particle size. To accomplish this, the X-Ray Diffraction (XRD) technique is employed to calculate the LS, peak shift (PS), Debye temperature (DT), Debye-Waller factor (DWF), and amplitude of vibrations (AV) of Fe3C. Key parameters, such as Debye temperature, amplitudes of vibration, Debye-Waller factor, lattice parameters, particle size, lattice strain, and vacancy formation energies, were determined. Notably, we estimated vacancy formation energies for Fe3C nanoparticles using X-ray Debye temperatures. Additionally, the synthesized ferrite powders were incorporated into polymer matrices to study their potential applications in composite materials, investigating aspects such as mechanical properties, thermal stability, and magnetic behavior.

n

n

n

Keywords: Fe3C, XRD, SEM, particle size, lattice strain, Debye-Waller factor and vacancy formation energy.

n[if 424 equals=”Regular Issue”][This article belongs to Journal of Polymer and Composites(jopc)]

n

[/if 424][if 424 equals=”Special Issue”][This article belongs to Special Issue under section in Journal of Polymer and Composites(jopc)][/if 424][if 424 equals=”Conference”]This article belongs to Conference [/if 424]

n

n

n

How to cite this article: Purushotham Endla, Endla AkhilBalaji Investigations into the Mechanical and Thermal Properties of Fe3C Compound: A Comprehensive Analysis jopc ; :-

n

How to cite this URL: Purushotham Endla, Endla AkhilBalaji Investigations into the Mechanical and Thermal Properties of Fe3C Compound: A Comprehensive Analysis jopc {cited };:-. Available from: https://journals.stmjournals.com/jopc/article=/view=0

n


n[if 992 equals=”Open Access”] Full Text PDF Download[else] nvar fieldValue = “[user_role]”;nif (fieldValue == ‘indexingbodies’) {n document.write(‘Full Text PDF‘);n }nelse if (fieldValue == ‘administrator’) { document.write(‘Full Text PDF‘); }nelse if (fieldValue == ‘jopc’) { document.write(‘Full Text PDF‘); }n else { document.write(‘ ‘); }n [/if 992] [if 379 not_equal=””]n

Browse Figures

n

n

[foreach 379]n

n[/foreach]n

nn

n

n[/if 379]n

n

References

n[if 1104 equals=””]n

 

  • Sathiyavimal, S. et al.Green chemistry route of biosynthesized copper oxide nanoparticles using Psidium guajava leaf extract and their antibacterial activity and effective removal of industrial dyes.  Environ. Chem. Eng. 9, 105033 (2021).
  • Jamzad, M. & Bidkorpeh, M. K. Green synthesis of iron oxide nanoparticles by the aqueous extract of Laurus nobilis leaves and evaluation of the antimicrobial activity. J. Nanostruct. Chem.10, 193–201 (2020).
  • Devatha, C., Jagadeesh, K. & Patil, M. Effect of Green synthesized iron nanoparticles by Azardirachta indicain different proportions on antibacterial activity.  Nanotechnol. Monit. Manag. 9, 85–94 (2018).
  • Ansari, M. A. & Asiri, S. M. M. Green synthesis, antimicrobial, antibiofilm and antitumor activities of superparamagnetic γ-Fe2O3NPs and their molecular docking study with cell wall mannoproteins and peptidoglycan.  J. Biol. Macromol. 171, 44–58 (2021).
  • Sadhasivam, S., Vinayagam, V. & Balasubramaniyan, M. Recent advancement in biogenic synthesis of iron nanoparticles.  Mol. Struct.1217, 128372 (2020).
  • Ansari, M. A. & Asiri, S. M. M. Green synthesis, antimicrobial, antibiofilm and antitumor activities of superparamagnetic γ-Fe2O3NPs and their molecular docking study with cell wall mannoproteins and peptidoglycan.  J. Biol. Macromol. 171, 44–58 (2021).
  • Murgueitio, E. et al.Green synthesis of iron nanoparticles: Application on the removal of petroleum oil from contaminated water and soils.  Nanotechnol. 2018, 1–8 (2018).
  • Vasantharaj, S., Sathiyavimal, S., Senthilkumar, P., LewisOscar, F. & Pugazhendhi, A. Biosynthesis of iron oxide nanoparticles using leaf extract of Ruellia tuberosa: Antimicrobial properties and their applications in photocatalytic degradation.  Photochem. Photobiol. B Biol.192, 74–82 (2019).
  • Vasantharaj, S., Sathiyavimal, S., Senthilkumar, P., LewisOscar, F. & Pugazhendhi, A. Biosynthesis of iron oxide nanoparticles using leaf extract of Ruellia tuberosa: Antimicrobial properties and their applications in photocatalytic degradation.  Photochem. Photobiol. B Biol.192, 74–82 (2019).
  • Jamzad, M. & Bidkorpeh, M. K. Green synthesis of iron oxide nanoparticles by the aqueous extract of Laurus nobilis leaves and evaluation of the antimicrobial activity. J. Nanostruct. Chem.10, 193–201 (2020).
  • Ansari, M. A. & Asiri, S. M. M. Green synthesis, antimicrobial, antibiofilm and antitumor activities of superparamagnetic γ-Fe2O3NPs and their molecular docking study with cell wall mannoproteins and peptidoglycan.  J. Biol. Macromol. 171, 44–58 (2021).
  • Kirdat, P. et al.Synthesis and characterization of ginger ( officinale) extract mediated iron oxide nanoparticles and its antibacterial activity. Mater. Today Proc. 43, 2826–2831 (2021).
  • Salgado, K. Márquez, O. Rubilar, D. Contreras, and G. Vidal, “The effect of phenolic compounds on the green synthesis of iron nanoparticles (FexOy-NPs) with photocatalytic activity,” Applied Nanoscience, vol. 9, pp. 371–385, 2019.
  • Šutka, M. Vanags, A. Spule et al., “Identifying iron-bearings nanoparticles precursor for thermal transformation into the highly active hematite photo-fenton catalyst,” Catalyst, vol. 10, p. 778, 2020.
  • A. Demirezen, S. Yilmaz, and D. D. Yilmaz, “Green synthesis and characterization of iron nanoparticles using aesculus hippocastanum seed extract,” International Journal of Advances in Science Engineering and Technology, vol. 6, 2 pages, 2018.
  • Azizi, A. Green synthesis of Fe3O4 nanoparticles and its application in preparation of Fe3O4/cellulose magnetic nanocomposite: A suitable proposal for drug delivery systems.  Inorg. Organomet. Polym. Mater.30, 3552–3561 (2020).
  • Nabati Souha, L., Alebrahim, M. T., Habibi Yangjeh, A. & Feizpoor, S. Green synthesis of iron oxide nanoparticles (Fe3O4) by extract of aerial organs of Russian knapweed (Acroptilon repens L.).  Mol. Res. (Iranian J. Biol.(2021).
  • Alabdallah, N. M. et al.Green synthesized metal oxide nanoparticles mediate growth regulation and physiology of crop plants under drought stress. Plants 10, 1730 (2021).
  • Noor, R. et al.Comparative analysis of iron oxide nanoparticles synthesized from ginger (Zingiber officinale) and cumin seeds (Cuminum cyminum) to induce resistance in wheat against drought stress. Chemosphere 292, 133201 (2022).
  • Inagaki, H. Furuhashi, T.Ozeki et al., J Mater Sci.6,1520 (1971).
  • Inagaki, H.Furuhashi, T.Ozeki &S.Naka, J.Mater, Sci.8,312 (1973).
  • B.Sirdeshmukh, K.G.Subhadra, K.A.Hussain, N.Gopi Krishna, B.Raghave-ndra Rao, Cryst.Res.Technol, 28,15 (1993)
  • Gopi Krishna and D.B.Sirdeshmukh, Indian J Pure & Appl Phys.31, 198 (1993).
  • Gopi Krishna et al, Indian J Phys. 84(7), 887 (2010).
  • R.Chipman and A.Paskin,J.Appl. Phys. 30,1938 (1959).
  • Gopi Krishna, D.B.Sirdeshmukh, B.Rama Rao, B.J.Beandry and K.A.Jr.Gsch-neidner,Indian J Pure & Appl Phys.24, 324 (1986).
  • W.James, The optical principles of the diffraction of x-rays (Bell and Sons, London, 1967).
  • International tables for X ray crystallography, Vol.III(Kynoch press, Birmingham) (1968).
  • Bharati, R., Rehani, P.B., Joshi, Kirit N., Lad and Arun Pratap, Indian Journal of Pure and Applied Physics, 44, (2006) 157-161.
  • Wilson, A.J.C.,(1949).X-rayOptics(Methuen, London).
  • Kaelble, E.F., Handbook of X-rays (New York Mc Graw ill) (1967)
  • F.Vetelino, S.P.Gaur, S.S.Mitra, Phys. Rev. B5, 2360 (1972).
  • R.Glyde, J.Phys and Chem Solids (G.B), 28, 2061 (1967).
  • Micro-and Macro-Properties of Solids, Springer Series in Material Science, (2006).
  • Purushotham, E. “Chemical Papers.” Springer Nature, vol. 76, pp. 7327–7331, 2022.
  • Purushotham, E. “Evaluation of Debye temperatures of α-phase copper–zinc alloys by using X-Ray diffraction method.” Materials Today Proceedings, vol. 46, no. 12, pp. 5922–5926, 2021
  • Purushotham, E. “Root mean square amplitudes of vibration and associated Debye temperatures of beryllium, scandium, and ruthenium.” Materials Today: Proceedings, vol. 47, no. 15, pp. 5034–5037, 2021.
  • Purushotham, E., & Veerati Radhika. “Materials Today: Proceedings.” Elsevier, vol. 47, no. 15, pp. 4993–4995, 2021.
  • Purushotham, E. “X-Ray Determination of Debye Temperature and Microhardness of Some Hexagonal Close Packed Elements Re, Os and Tl.” IOP Conference Series: Materials Science and Engineering, vol. 1119, p. 012001, 2021.
  • Purushotham, E. “Characterization of size-dependent thermal properties in strained nanocrystalline powder using Williamson-Hall.” IOP Conference Series: Materials Science and Engineering, vol. 981, p. 022086, 2020.

nn[/if 1104][if 1104 not_equal=””]n

    [foreach 1102]n t

  1. [if 1106 equals=””], [/if 1106][if 1106 not_equal=””],[/if 1106]
  2. n[/foreach]

n[/if 1104]

nn


nn[if 1114 equals=”Yes”]n

n[/if 1114]

n

n

[if 424 not_equal=””][else]Ahead of Print[/if 424] Open Access Original Research

n

n

n

n

n

Journal of Polymer and Composites

n

[if 344 not_equal=””]ISSN: 2321–2810[/if 344]

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

n

Volume
[if 424 equals=”Regular Issue”]Issue[/if 424][if 424 equals=”Special Issue”]Special Issue[/if 424] [if 424 equals=”Conference”][/if 424]
Received March 1, 2024
Accepted March 8, 2024
Published

n

n

n

n

n

nn function myFunction2() {n var x = document.getElementById(“browsefigure”);n if (x.style.display === “block”) {n x.style.display = “none”;n }n else { x.style.display = “Block”; }n }n document.querySelector(“.prevBtn”).addEventListener(“click”, () => {n changeSlides(-1);n });n document.querySelector(“.nextBtn”).addEventListener(“click”, () => {n changeSlides(1);n });n var slideIndex = 1;n showSlides(slideIndex);n function changeSlides(n) {n showSlides((slideIndex += n));n }n function currentSlide(n) {n showSlides((slideIndex = n));n }n function showSlides(n) {n var i;n var slides = document.getElementsByClassName(“Slide”);n var dots = document.getElementsByClassName(“Navdot”);n if (n > slides.length) { slideIndex = 1; }n if (n (item.style.display = “none”));n Array.from(dots).forEach(n item => (item.className = item.className.replace(” selected”, “”))n );n slides[slideIndex – 1].style.display = “block”;n dots[slideIndex – 1].className += ” selected”;n }n”}]