Open Access
Dr. Purushotham Endla,
Endla Akhil Balaji,
- Associate Professor, Department of Physics, School of Sciences, SR University, Telangana, India
- B.Tech Student, Computer Science and Engineering, Kakatiya Institute of Technology and Science, Telangana, India
Abstract
This research paper presents a comprehensive investigation into transforming micro-sized silver (Ag) powder into nanostructured Ag powder by applying high-energy ball milling. The ball milling process was executed over a total duration of 20 hours, with periodic sampling every 4 hours to monitor the evolving characteristics of the material. The particle size, lattice strain, Debye-Waller factor, and root mean square amplitudes of vibration were calculated by using X-ray powder diffraction techniques. Notably, a noteworthy observation emerged in this study: a discernible increase in the Debye-Waller factor was observed about lattice strain, indicating a previously unidentified correlation. The correlation between lattice strain and the influential Debye-Waller factor, this paper successfully estimated Debye-Waller. From the correlation between the strain and effective Debye- Waller factors have been estimated for Ag. The results of this research contribute to the fundamental understanding of the mechanical transformation of micro-sized Ag powder into nanostructured Ag powder and the implications for its physical properties.
Keywords: XRD, lattice strain, particle size, Debye-Waller factor, Debye temperature, applications.
[This article belongs to Special Issue under section in Journal of Polymer and Composites (jopc)]
Dr. Purushotham Endla, Endla Akhil Balaji. Nanocrystalline Silver: Synthesis by High-Energy Ball Milling, X-ray Debye Temperature Analysis, and Diverse Applications. Journal of Polymer and Composites. 2024; 11(12):140-148.
Dr. Purushotham Endla, Endla Akhil Balaji. Nanocrystalline Silver: Synthesis by High-Energy Ball Milling, X-ray Debye Temperature Analysis, and Diverse Applications. Journal of Polymer and Composites. 2024; 11(12):140-148. Available from: https://journals.stmjournals.com/jopc/article=2024/view=133122
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Journal of Polymer and Composites
Volume | 11 |
Special Issue | 12 |
Received | 30/10/2023 |
Accepted | 12/12/2023 |
Published | 17/02/2024 |