Preparation and Characterization of TiO2 Nanoparticles by Green Method

Open Access

Year : 2023 | Volume :11 | Special Issue : 02 | Page : 61-67
By

    Rasha Tariq Salim

  1. Dunya Edan AL-Mammar

  1. Student, College of Science, University of Baghdad, Baghdad, Iraq
  2. Professor, Department of Chemistry,College of Science, University of Baghdad, Baghdad, Iraq

Abstract

In this study, we attempted to synthesize TiO2 nanoparticles utilizing titanium tetrachloride as a precursor and an aqueous extract of Sansevieria plant leaves. Atomic force microscopy (AFM), X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy, and Brunauer-Emmett-Teller (BET) analysis were used to identify the synthesized TiO2 nanoparticles As per the surface topography, the average diameter of nanoparticles is considered as 67.73 nm. Debye-Scherrer equation was used to summarize the size of the crystals, the result shows that the average crystalline size for TiO2 sample was 15.2 nm. Few spherical, non-agglomerated particles could be seen in the SEM image of TiO2 nanoparticles. The appearance of the bending vibrations of Ti-O and Ti-O-Ti are shown at 688.59, 497.63, and 950.91 cm–1, respectively, demonstrating the presence of TiO2 nanoparticles. BET equation was used to estimate the porosity and surface area for the prepared sample.

Keywords: Green method, Sansevieria, titanium dioxide nanoparticles

This article belongs to Special Issue Conference Material Science and Nanotechnology

How to cite this article: Rasha Tariq Salim, Dunya Edan AL-Mammar Preparation and Characterization of TiO2 Nanoparticles by Green Method jopc 2023; 11:61-67
How to cite this URL: Rasha Tariq Salim, Dunya Edan AL-Mammar Preparation and Characterization of TiO2 Nanoparticles by Green Method jopc 2023 {cited 2023 Jun 28};11:61-67. Available from: https://journals.stmjournals.com/jopc/article=2023/view=111739

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Conference Open Access Original Research
Volume 11
Special Issue 02
Received December 8, 2022
Accepted January 31, 2023
Published June 28, 2023