Bharat Raval,
Paresh V. Dalal,
Rajesh Kumar Katare3,
- Teacher Department of Physics, Seva Sadan Mahavidhyalay ,Burhanpur Madhya Pradesh India
- Vice Principle Department of Physics, V.S. Naik College Raver, Jalgaon Maharashtra India
- Professor Department of Physics, SAGE University Indore, Indore Madhya Pradesh India
Abstract
Barium tartrate chargers were synthesized using the gel system with a single prolixity fashion at room temperature in a 1 w/ v agar- agar gel as the growth medium. The reactants, 1M BaCl₂ (dihydrate) and 1M disodium tartrate, were introduced into the gel and allowed to interact for a period of 25 days. Completely developed white, candescent, spherulitic-structured chargers of barium tartrate were gathered later. Infrared spectroscopy( FTIR) revealed characteristic peaks at 3065.7, 2875.6, and 2735.9 cm- 1 indicating hydration water, a peak at 1589 cm- 1 corresponding to free carbonyl stretching,1382.8 cm- 1 due to> C =O symmetric vibration, and peaks at 751.1 and 689.6 cm- 1 indicating essence- oxygen stretching. The maximum weight of a single demitasse reached roughly 95 mg, showing well- defined morphology. X-ray diffraction (XRD) analysis verified the liquid nature of the samples, revealing an orthorhombic demitasse system with a unit cell volume of 5671 Å ³. Thermal analysis( TGA and DTA) supported the presence of water moves within the demitasse chassis, with dehumidification being around 306 ℃ and corruption into oxide observed between 400 to 600 ℃. This study represents the first reported case of pure barium tartrate chargers grown in agar- agar gel, as substantiated by the absence of previous literature on this content.
Keywords: Agar- agar gel, Crystal growth, Barium Tartrates, FTIR, XRD, TGA, DTA.
[This article belongs to International Journal of Universe(iju)]
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Volume | 01 |
Issue | 01 |
Received | July 19, 2024 |
Accepted | August 7, 2024 |
Published | August 31, 2024 |