Electro-chemical treatment of graphite oxide: preparation and Characterization of high quality Graphene material

Open Access

Year : 2024 | Volume : | : | Page : –
By

Vishwa Deepak Dwivedi,

Pradeep Kumar Singh,

Pankaj Kumar Singh,

  1. Research Scholar Micro-nano Development Research Center, Department of Mechanical Engineering, GLA University Mathura Uttar Pradesh India
  2. Assistant Professor Micro-nano Development Research Centre, Department of Mechanical Engineering, GLA University Mathura Uttar Pradesh India
  3. Assistant Professor Micro-nano Development Research Centre, Department of Mechanical Engineering, GLA University Mathura Uttar Pradesh India

Abstract

With the enlargement of flexibility and suitability in material industries, high-performance thermal management materials are demanded with high thermal conductivity and electrical insulation are growing. In recent years, graphene has received a numerous focus from science community due to its high thermal conductivity and electrical insulation. Fabrication of light weight graphene and its derivatives as graphene Oxide (GO) and reduced graphene oxide (rGO) via facile processing method is yet a challenge for industries. The preparation of graphene through the wet exfoliation process of graphite leads to a several outstanding features of graphene. By thermal chemical reduction method, is simple and ecofriendly process used for the intercalate of graphene from graphite in a mass amount in the presence of aqueous solution H2SO4 and H2O2 through electrolysis process at high voltage (60 Volt) with electrolyte heating approach (60-70oC). This study investigates the structure and composition of graphene produced at different temperature as 650oC, 750oC and 850oC by thermal reduction of graphene oxide (GO) for short range of time (5 minutes). Thermal reduced graphene oxide (TrGO) diffraction peak, inter planar distance, crystallite size and structural disorder are all the significantly impacted by magnetic field and cyclic thermal loading, according to the FESEM and Raman spectra. TEM, UV analysis and TGA analyses demonstrated the significant influence of magnetic field and cyclic heating loading on the surface topography and micro structural characteristics. The thermal stability and functional groups contain oxygen seem to be unaffected by the magnetic field and cyclic thermal loading.

Keywords: Thermally reduced graphene oxide, Electro chemical exfoliation, electrolyte, thermal reduction, Green synthesis.

How to cite this article: Vishwa Deepak Dwivedi, Pradeep Kumar Singh, Pankaj Kumar Singh. Electro-chemical treatment of graphite oxide: preparation and Characterization of high quality Graphene material. Journal of Polymer and Composites. 2024; ():-.
How to cite this URL: Vishwa Deepak Dwivedi, Pradeep Kumar Singh, Pankaj Kumar Singh. Electro-chemical treatment of graphite oxide: preparation and Characterization of high quality Graphene material. Journal of Polymer and Composites. 2024; ():-. Available from: https://journals.stmjournals.com/jopc/article=2024/view=155421

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Ahead of Print Open Access Original Research
Volume
Received June 7, 2024
Accepted June 24, 2024
Published July 5, 2024
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